Fruit growing
and viticulture of South Russia

Annotation

The article considers the relevance of creating an electronic database of quality indicators of authentic red wines produced in the Krasnodar region. The database contains information on the physicochemical parameters of high-quality red wines produced in the Krasnodar region, of the following categories: wines with a protected geographical indication (PGI), with the designation of the region of production; wines with a protected appellation of origin (PAO), indicating the vineyard/small area of production (municipality, rural settlement); wines with the prospect of being registered as wines with PGI or PAO. Information about the producer, the name of the wine, the varietal composition of grapes and the year of harvest is presented. The physicochemical parameters of wines are represented by the mass concentration of inorganic cations (K+ , Na+ , Mg2+, Ca2+) and anions (Cl� , SO4 2- ) � obtained using the method of high-performance capillary electrophoresis (HPCE) on the �apel 105M device (Russia); microelements (Sr, Rb, Ti) using the method of atomic absorption spectroscopy on the Kvant.Z device (Russia); phenolic substances, including anthocyanins using the spectrometry method; as well as chromatic characteristics and their calculated indicators (intensity, shade, yellowness and color coordinates in the CIELab system). The proposed database contains empirical data obtained by scientists of the scientific center "Winemaking" and the Center for Collective Use of High-Tech Equipment of the FSBSI NCFSCHVW in 2020-2022. As a result of the research and development of a database of quality indicators of authentic red wines produced in the Krasnodar region, a certificate of state registration No. 2022620910 dated 04.21.2022 was obtained. The database i s intended for the accumulation, operational search, storage and analysis of information, and also creates the basis for the development of a quality control system for wine products with geographical affiliation

Annotation

The article presents the results of identifying the processes of transformation of nisin in wine during interaction with bentonites of various manufacturers. An attempt is made to study the mechanisms of interaction of the nisin antibiotic with mineral sorbents of various deposits by identifying the relative degree of its removal, as well as to establish the effect of technological processing of bentonite clays the composition of inorganic cations and organic acids in wines. With the addition of nisin, the amount of ammonium, potassium, and magnesium decreased, which is possibly due to the binding ability of nisin with respect to these cations due to its polypeptide structure. It was experimentally established that when the Nizin preparation was introduced and the wine was treated with bentonite clays, the difference between the average values of the mass concentrations of organic acids in wine was not statistically significant. It was found that the processing of white table wine with the addition of nisin by bentonite clays as a whole showed a high degree of nisin removal � more than 80 %. It was found that the degree of dispersion (particle size) of bentonites did not significantly affect their sorption ability relative to the nisin. The external and internal factors as activators and inhibitors of adsorption � for the removal of nisin are analyzed. It has been suggested that the interaction of nisin with bentonites occurs mainly due to electrostatic reactions, and not due to adhesion forces that increase with decreasing sorbent particle size. The possible mechanisms of nisin sorption in the process of its detection in the wines are proposed. It is recommended to use the bentonite clays of Bentovin (Dash-Salakhninskoye deposit, Republic of Azerbaijan), Vinobent (Mine "10th farm", Khakassia) for ensuring the consumer safety of wines containing the residual amounts of nisin.

Annotation

The influence of grape dietary fibers on decontamination of natamycin in wine has been studied. Grape dietary fibers obtained from sweet pomace of Chardonnay grapes and fermented grapes � Krasnostop Anapskiy, Cabernet Sauvignon and Merlo were used for the studies. The mass fraction of fiber in the presented fiber samples ranged from 57.2 � 2.9 (Cabernet Sauvignon) to 65.3 � 3.3 % (Chardonnay), the electrokinetic potential � from minus 26 � 3 (Chardonnay) to minus 49 � 5 mV (Krasnostop Anapskiy). Studies were carried out on a model mixture of dry white wine with 10 mg/dm3 of introduced natamycin. Influence of time of contact of wine with fibers and their amount on sorption of natamycin was established. It was revealed that the maximum sorption of natamycin occurs when in contact with fibers during the first 2 hours, so further maintenance of them is impractical. The addition of the fibers to the wine in an amount of 3.0 g/dm3 resulted in the removal of natamycin from 42 to 68 %. Fibers obtained from white Chardonnay grape pomace contributed to less sorption of natamycin, and from red pom-ace of Krasnostop Anapskiy grape variety � more, which correlates with values of electrokinetic potential on the surface of the fibers. It is assumed that for the complete decontamination of natamycin it is necessary to use combined treatments with other sorbents having a negative charge of active centers on the surface.

Annotation

Quality improvement and improvement of organoleptic characteristics of cognac in its production is achieved mainly due to the extraction of oak wood components, their transformation to aromatic aldehydes and tannins and their accumulation in the mature cognac distillate in optimal concentrations. The method of preparation of oak wood is an important technological technique that has a great impact the quality of cognac. When processing the wood, the dissolution of some of the components of the cell walls occurs, which leads to an increase in the volume of cell cavities, and, as a consequence, to an increase in porosity. Increased porosity and increased permeability of the cell wall of wood fibers provides a more complete extraction of lignin, tannins and aromatic aldehydes by distillate in the mature process of cognac distillation. At the same time, respectively, the mechanical properties of wood are changed. The article presents the results of studies of changes in the adsorption capacity (porosity) of oak wood using the different ways of its activation: acid, alkaline, thermal and biochemical activation. It is established that alkaline treatment leads to the strongest changes in the structure of oak wood, by increasing the adsorption capacity (porosity) by 4,7-5,6 times. In the process of heat treatment of oak wood the value of adsorption on its surface increases in 4,4 times, and at biochemical treatment � in 2,4-3,7 times in comparison with untreated wood. Acid treatment of oak wood was characterized by the lowest adsorption value among all the considered ways of treatments, increasing in the adsorption value by only 2,2-3 times.

Annotation

New knowledge was obtained about the conformity to natural lows of changes in physicochemical and organoleptic indicators of wine production in the presence of a preservation of microbial origin of nisin (food supplement E234), which will become the basis for the technological foundation of additional processing of sorbents for wine materials aimed to increasing in their consumer safety and quality. It was established in the process of research that in the experimental samples of wine with the addition of nisin all analyzed parameters ( volume fraction of ethyl alcohol, mass concentration of sugars, mass concentration of titrated acids in terms of tartaric acid, mass concentration of volatile acids in terms of acetic acid, mass concentration of the above extract, mass concentration of citric acid, mass concentration of total sulfur dioxide, organic acids, phenolic compounds, including anthocyanins for red wines) the physical-chemical composition of the test samples of wines remained unchanged, and remained at the same level as in the control samples. Study carried out of white and red wines with the addition of nisin showed that during the aging the typical oxidation-reduction processes are occurred typical to the wine aging process. The most significant was the change in the mass concentration of organic acids, which mainly affects the taste and, consequently, the quality of the wine. As a result of the analysis of experimental data, it was established that the control and testing samples had the same organoleptic characteristics and tasting score. Dry white table wine has a straw color, pure wine aroma with flower shades, corresponding to wine type; full harmonious fresh taste, without extraneous shades.